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NMRFAM “Vosges” Avance HD 600III


Vosges is a Bruker Avance HD (ex. Agilent) NMR system 600 MHz, 14.1 T standard bore magnet NMR spectrometer. This instrument is equipped with a TCI (H/F-CN-D) cryogenic probe. The CryoProbe is designed for highest sensitivity on 1H, 19F, and 13C (with cold preamplifiers for 1H/19F, 13C, and 2H), providing added 19F detection and decoupling capability with the performance of a dedicated fluorine CryoProbe. The probe is compatible with shaped tubes for optimum performance on lossy samples.

Console Capabilities

Vosges is equipped with three fully independent channels (plus lock channel) for 19F{1H} and 1H{19F} experiments, and simultaneous decoupling on multiple nuclei such as 13C, 15N, and 19F. A deuterium channel is provided for lock and deuterium decoupling (cooled 2H preamplifier provides increased stability).

Linear amplifiers for the RF channels are one 100 W (1H/19F, 550-600 MHz), two 500 W (13C,15N, 6-220 MHz), and one 150W (2H). Pulsed field gradient capability is provided by an actively shielded single axis Z-gradient PFG module. Vosges includes two amplifiers for the future solids probe: 500W (1H) and 50 W (X-channel). 

The temperature range for the cryoprobe is -40 to 80 C.

Available Probes

  • 5 mm z-axis pulsed field gradient triple resonance Cold probe (1H/19F{13C,15N, 2D})
  • 5 mm triple-axis pulsed field gradient triple resonance RT probe (1H{13C,15N})

Cost

The base rate for time on this machine is $8.00/hour for publishable work and $250/hour for proprietary work.

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Donate to NMRFAM. US tax-deductible donation can be made to NMRFAM
Please write check payable to "UW Foundation, Account 112152802"  
And mail to: 
Attn: Sarah Lynn Traver Saunders
Associate Administrative Program Specialist 
University of Wisconsin-Madison 
433 Babcock Drive 
Madison, WI 53706 
Tel: 608-265-2507 or email 

 

1st: Lai Bergeman 
Rm 171; Phone 262-3173

2nd: Milo Westler
Rm B160; Phone 263-9599

3rd: Paulo F. Cobra
Rm B224; Phone 265-3303

4th: Marco Tonelli
Rm B160; Phone 263-9493

5th: John Markley
Rm 171A; Phone 263-9349

We welcome your questions and feedback!

NMRFAM Established 1987