September 2009 |

September 2009

This announcement is to remind you that September 19^th @ 4pm is the deadline for requesting spectrometer time in October 2009 at NMRFAM.

Visit our website @ www.nmrfam.wisc.edu and check the News on the right side.
The ¹³C/¹⁵N direct observe cryogenic probe has been installed on Kerry (500I)- a 500 MHz Bruker Avance III with Samplejet. The signal-to-noise for ¹³C is 1400:1 (ASTM) and for ¹⁵N 80:1 (formamide). It is still suitable for ¹H observation (S/N 1600:1 Ethylbenzene). This spectrometer is available for users.
A Bruker Avance III 600 MHz LC-MS-NMR and a 700 MHz NMR spectrometer are on order. They are expected to be delivered early 2010. The 600 MHz spectrometer will have a LC-MS system for characterization and isolation of metabolites and natural products and will be delivered with 5mm ¹H{¹³C/¹⁵N/³¹P} and 1.7mm ¹H{¹³C/¹⁵N} cryogenic probes. The 700 MHz instrument will have a 5mm ¹H{¹³C/¹⁵N/³¹P} cryogenic probe. Both systems will have SampleJet sample changers.
See the YouTube videos describing rNMR, the new small molecule visualization and quantification tool.

Instrument	Cow name	Shortcut name	Probe^(a)	Status (09/11/2009)
Varian VNS 900	Fleckvieh	900	c-tr	OK (cold ¹H and ¹³C preamps)
Varian VNS 800	Gelbvieh	800	c-tr	OK
Bruker DMX 750	Telemark	750	c-tr	under repair
Bruker DMX 600	Dexter	600 I	c-tr	OK
Varian VNS 600	Jaulan	600 II	c-tr	OK
Bruker Avance 500	Kerry	500 I	Multiple	OK- Avance III console with ¹³C/¹⁵N observe cryogenic probe & SampleJet
Bruker DMX 500	Devon	500 II	c-tr	OK
Bruker DMX 400	Pisa	400	Multiple	OK
^(a) rt - room temperature; c - cryogenic; tr - ¹H{¹³C,¹⁵N} triple resonance; multiple - multiple probes; VNS- Varian Direct Drive; console Avance- Bruker Avance III console

To sign up for time: Use Sundial at www.sesame.wisc.edu/Sundial/sundial_main.html. Contact Anne Lynn Gillian-Daniel (gillian@nmrfam.wisc.edu, 608-262-3173) for assistance.

Please visit the NMRFAM website for more information about NMRFAM.