3D TROSY-HN(CO)CACB - with
minimal H2O saturation and
optional 2H decoupling. This program uses the
gp gradient syntax.
Yang and Kay, J. Am. Chem. Soc. 1999, 121, 2571-2575.
Include file for optional expt time correction: faexptcorr.incl
Shaped pulse file for Ca rectangular shaped pulse:
fasqua.256.jc (JCAMP-DX).
Read more about the pulse shape
file formats.
Acquisition parameters: 750 MHz
Use ux2flx or
equivalent utility to convert your Bruker data to Felix "dat" format.
Felix95/98 processing macro: ft3d_hncocacbtr.mac
Also used (for correction of digital filter artifacts): digphs.mac
References
Acquisition
Pulse program
Include files etc.
Shaped pulse file for EBURP-1 shaped pulse:
eburp1.512.jc (JCAMP-DX).
Shaped pulse file for REBURP shaped pulse:
reburp.256.jc (JCAMP-DX).
Shaped pulse file for GaussCascadeG3 shaped pulse:
g3.256.fa.jc (JCAMP-DX).
Parameters
Processing