3D HNCO - with Watergate reverse INEPT (FHSQC) and minimal H2O saturation


3D HNCO - with Watergate reverse INEPT (FHSQC) and minimal H2O saturation. This program uses the gp gradient syntax. Optimized for CryoProbe use.

References

Kay, Xu, and Ymazaki, J. Magn. Reson. A 10l, 129-133 (1994)

Mori et al., J. Magn. Reson. B 108, 94-98 (1995)

Sklenar, Piotto, Leppik, and Saudek: J. Magn. Reson. A 102, 241-245 (1993)

Acquisition

Pulse program

hncof.fa

Include files etc.

Include file for optional expt time correction: faexptcorr.incl

Composite pulse decoupling program for SEDUCE-1 decoupling: waltz16sp3

Shaped pulse file for SEDUCE-1 decoupling: seduce1.jc (JCAMP-DX), seduce1.rf (binary RF format) or seduce1.txt (ASCII).

Read more about the pulse shape file formats.

Parameters

Acquisition parameters: 500 MHz

Processing

Use ux2flx or equivalent utility to convert your Bruker data to Felix "dat" format.

Felix95 processing macro: ft3d_hncof.mac

Also used (for correction of digital filter artifacts): digphs.mac


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