3D TROSY-HNCO - with Watergate reverse INEPT
(3-9-19) and minimal H2O saturation.
This program uses the gp gradient syntax. Optimized for CryoProbe use.
Yang and Kay, J. Biomol. NMR. 13, 3-10 (1999) (experiment 2b in this paper)
with modifications from Yang and Kay, J. Biomol. NMR. 14, 273-276 (1999).
Include file for optional expt time correction: faexptcorr.incl
Shaped pulse file for Ca rectangular shaped pulse:
fasqua.256.jc (JCAMP-DX).
Read more about the pulse shape
file formats.
Acquisition parameters: 750 MHz
Use ux2flx or
equivalent utility to convert your Bruker data to Felix "dat" format.
Felix95/98 processing macro: ft3d_hncotrk2b.mac
Also used (for correction of digital filter artifacts): digphs.mac
References
Acquisition
Pulse program
Include files etc.
Shaped pulse file for EBURP-1 shaped pulse:
eburp1.512.jc (JCAMP-DX).
Parameters
Processing