3D TOCSY 13C-1H constant-time
sensitivity enhanced HSQC
with optional 13C' decoupling. Use optional
15N decoupling with 15N labeled samples.
Vuister and Bax, J. Magn. Reson., 98, 428-435 (1992)
Schleucher et al., J. Biol. NMR, 4, 301-306 (1994)
Gradient program: fatoccthsqcse.r
Include file for pulsed field gradient definitions: Gradfa.incl
Shaped pulse file for SEDUCE-1 shaped 13C' pulse:
seduce1.jc (JCAMP-DX),
seduce1.rf (binary RF format) or
seduce1.txt (ASCII).
Read more about the pulse shape
file formats.
Acquisition parameters - 500 MHz: n/a
Use ux2flx or
equivalent utility to convert your Bruker data to Felix "dat" format.
Felix95 processing macro: ft3d_se.mac
Also used (for correction of digital filter artifacts): digphs.mac
References
Acquisition
Pulse program
Gradient program
Include files etc.
Parameters
Processing